Journal of Chromatography & Separation Techniques
Open Access

Synthesis and structural elucidation of Ni (II), Cu (II), Zn (II) and Cd (II) metal complexes of oxazoline based ligands

International Summit on Current Trends in Mass Spectrometry

July 13-15, 2015 New Orleans, USA

Muluye Melak Zeneb

Posters-Accepted Abstracts: J Chromatogr Sep Tech

Abstract :

Synthesis of 2-(2â??-hydroxyphenyl)-2-oxazoline(2-Phox) and 2-(4-hydroxyphenyl)-2-oxazoline(4-Phox) and their complexes with Ni (II), Cu (II), Zn (II) and Cd (II) have been done. They have been characterized by elemental analysis, magnetic susceptibility, NMR (HH-COSY, HSQC, HMBC), UV-vis, IR spectroscopy and conductance measurement. The complexes were formed in 1:2 (M: L) ratio. Their molar conductance of one millimolar solution measured in DMF indicated them to be nonelectrolyte. On the basis of these studies a tetrahedral geometry has been assigned for all the complexes.